N-叔丁氧羰基-L-谷氨酸 5-甲酯合成路线 （共 18 条）
反应条件
sodium carbonate in 1,4-dioxane; water
参考文献
More, Swati S.; Vince, Robert
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 13 p. 3793 - 3797
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C; P=2068.65 Torr; 2 h;
参考文献
Boudreault, Pierre-Luc; Voyer, Normand
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 9 p. 1459 - 1465
反应条件
triethylamine in 1,4-dioxane; water 4 h; Ambient temperature;
参考文献
El Marini; Roumestant; Viallefont; Razafindramboa; Bonato; Follet
Synthesis, 1992 , # 11 p. 1104 - 1108
反应条件
triethylamine in 1,4-dioxane; water
参考文献
Burkhart; Holbert; Metcalf
Tetrahedron Letters, 1984 , vol. 25, # 46 p. 5267 - 5270
反应条件
Candida antarctica lipase; phosphate buffer in methanol; hexane T=37°C; 48 h;
参考文献
Barbayianni, Efrosini; Fotakopoulou, Irene; Schmidt, Marlen; Constantinou-Kokotou, Violetta; Bornscheuer, Uwe T.; Kokotos, George
Journal of Organic Chemistry, 2005 , vol. 70, # 22 p. 8730 - 8733
反应条件
1: 97 percent / TMSCl / 20 °C 2: 91 percent / Na2CO3 / dioxane; H2O View Scheme
参考文献
Bhat, Ramakrishna G.; Porhiel, Emmanuel; Saravanan, Vadivelu; Chandrasekaran, Srinivasan
Tetrahedron Letters, 2003 , vol. 44, # 28 p. 5251 - 5253
反应条件
triethylamine in water; acetone 2 h;
参考文献
Jerumanis, Stanislas; Lefebvre, Jean
Bulletin des Societes Chimiques Belges, 1994 , vol. 103, # 3 p. 127 - 130
反应条件
1: triethylamine; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0.5 h / 0 - 20 °C / |Inert atmosphere 2: palladium 10 on activated carbon; hydrogen / methanol / 3 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Usuki, Toyonobu; Sugimura, Takanori; Komatsu, Akira; Koseki, Yohei
Organic Letters, 2014 , vol. 16, # 6 p. 1672 - 1675
反应条件
(i) MgCO3, aq. dioxane, (ii) /BRN= 1363586/; Multistep reaction;
参考文献
Anderson; Barton; Hardy; Kenner; Preston; Sheppard
Journal of the Chemical Society. Perkin transactions 1, 1967 , vol. 1, p. 108 - 113
反应条件
1: DCC / ethyl acetate / 1.) 0 deg C, 2.) 3 h, room temperature 2: NaBH4 / ethanol; tetrahydrofuran / 0.25 h / 0 °C 3: 92 percent / imidazole / dimethylformamide / 3 h / Ambient temperature 4: NaH / diethyl ether / 1.) 0 deg C, 2.) 18 h, room temperature View Scheme
参考文献
Shimamoto, Keiko; Ohfune, Yasufumi
Tetrahedron Letters, 1989 , vol. 30, # 29 p. 3803 - 3804
