3,4,5-三甲氧基苯甲酰氯合成路线 （共 203 条）
反应条件
1: 1.) ZnCl2 / 1.) Et2O, reflux, 3 h, 2.) benzene, r.t., overnight
2: 98percent hydrazine hydrate / ethanol / 5 h / Heating
3: KOH / 1 h / 180 °C
4: 72 percent / K / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Azzena, Ugo; Denurra, Teresa; Fenude, Emma; Melloni, Giovanni; Rassu, Gloria
Synthesis, 1989 , # 1 p. 28 - 30
反应条件
in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Kar
Pharmazie, 1983 , vol. 38, # 5 p. 313 - 315
反应条件
triethylamine in dichloromethane
0.5 h; Ambient temperature;
参考文献
Gaviraghi, G.; Nicola, M.; Pinza, M.; Pifferi, G.
Farmaco, Edizione Scientifica, 1980 , vol. 35, # 10 p. 801 - 811
