反应条件
1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 4 h / 20 °C
2: N-ethyl-N,N-diisopropylamine / acetonitrile / 2.5 h / 0 - 20 °C
3: hydrogenchloride / ethanol / 16 h / 50 - 55 °C
View Scheme
参考文献
Leahy, David K.; Desai, Lopa V.; Deshpande, Rajendra P.; Mariadass, Antony V.; Rangaswamy, Sundaramurthy; Rajagopal, Santhosh K.; Madhavan, Lakshmi; Illendula, Shashidhar
Organic Process Research and Development, 2012 , vol. 16, # 2 p. 244 - 249