1,1,3-三甲基环戊烷合成路线 (共 79 条)
反应条件
N-Pyrrolidinyllithium in tetrahydrofuran T=0°C;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
NaPPh2 in tetrahydrofuran T=25°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Ashby, E. C.; Gurumurthy, R.; Ridlehuber, R. W.
Journal of Organic Chemistry, 1993 , vol. 58, # 21 p. 5832 - 5837
反应条件
magnesium in tetrahydrofuran T=25°C; 8 h;
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
1: HCl / 2 °C 2: xylene / 40 °C View Scheme
参考文献
McKinley; Stevens; Baldwin
Journal of the American Chemical Society, 1945 , vol. 67, p. 1455,1458
Full Text Show Details
Gulf Research and Devel. Co.
Patent: US2415599 , 1944 ;
反应条件
para-dinitrobenzene; N-Pyrrolidinyllithium in tetrahydrofuran T=0°C; 12 h;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0°C; 72 h; Further byproducts given;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0°C; 72 h; Further byproducts given;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
lithium diisopropyl amide in diethyl ether T=0°C; Further byproducts given;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0°C; Further byproducts given;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0°C; Further byproducts given;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437