1,1,3-三甲基环戊烷合成路线 （共 79 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0°C; 20 h; Further byproducts given;
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Patil, Girish S.
Journal of Organic Chemistry, 1995 , vol. 60, # 3 p. 663 - 672
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 2 h / 25 °C 2: PCl5 / hexane / 24 h / 25 °C 3: 17 percent Chromat. / Mg, DCPH / tetrahydrofuran / 8 h / 25 °C View Scheme
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
参考文献
McKinley; Stevens; Baldwin
Journal of the American Chemical Society, 1945 , vol. 67, p. 1455,1458
Full Text Show Details
Gulf Research and Devel. Co.
Patent: US2415599 , 1944 ;
反应条件
1: 83 percent / LiAlH4 / diethyl ether / 18 h / 25 °C 2: pyridinium chlorochromate / CH2Cl2 / 2 h / 25 °C 3: PCl5 / hexane / 24 h / 25 °C 4: 17 percent Chromat. / Mg, DCPH / tetrahydrofuran / 8 h / 25 °C View Scheme
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
lithium diisopropyl amide in diethyl ether T=0°C; 48 h;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
1: PCl5 / hexane / 24 h / 25 °C 2: 17 percent Chromat. / Mg, DCPH / tetrahydrofuran / 8 h / 25 °C View Scheme
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=25°C; 30 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
magnesium in tetrahydrofuran T=25°C; 8 h; Further byproducts given;
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
magnesium in tetrahydrofuran T=25°C; 8 h; Further byproducts given;
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
magnesium in tetrahydrofuran T=25°C; 8 h; Further byproducts given;
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
