1: H2SO4 / Heating 2: LiAlH4 / diethyl ether 3: polyphosphoric acid / 1 h / 220 °C View Scheme
参考文献
Bendall,V.I.; Dharamshi,S.S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 2732 - 2734
1: LiAlH4 / diethyl ether 2: polyphosphoric acid / 1 h / 220 °C View Scheme
参考文献
Bendall,V.I.; Dharamshi,S.S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 2732 - 2734
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C / |Inert atmosphere 1.2: 5 h / 20 °C / |Inert atmosphere 2.1: [(2,4-t-BuPhO)3PAu(NCPh)]SbF6 / toluene / 1 h / 0 °C View Scheme
参考文献
McGonigal, Paul R.; De Leon, Claudia; Wang, Yahui; Homs, Anna; Solorio-Alvarado, Cesar R.; Echavarren, Antonio M.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 52 p. 13093 - 13096
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / |Inert atmosphere 1.2: 12 h / 23 °C / |Inert atmosphere 2.1: [MeCNAu((1,1′-biphenyl-2-yl)-di-tert-butylphosphine)]+SbF6− / 1,2-dichloro-ethane / 3 h / 120 °C / |Sealed tube; |Inert atmosphere View Scheme
参考文献
Wang, Yahui; McGonigal, Paul R.; Herle, Bart; Besora, Maria; Echavarren, Antonio M.
Journal of the American Chemical Society, 2014 , vol. 136, # 2 p. 801 - 809
Kayser
Annales de Chimie (Cachan, France), 1936 , vol. <11> 6, p. 145,176
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Tiffeneau; Levy; Kayser
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1933 , vol. 196, p. 1407
