反应条件
1: 60 percent / petroleum ether; toluene / 50 h / Irradiation
2: 80 percent / mCPBA / CHCl3 / 3 h / Ambient temperature
3: 1) LiAlH4, 2) PCC / 1) THF, reflux, 16 h, 2) CH2Cl2
View Scheme
参考文献
Sonawane, Harikisan R.; Naik, Vishwaniyant G.; Bellur, Nanjundiah S.; Shah, Virendra G.; Purohit, Pramod C.; et al.
Tetrahedron, 1991 , vol. 47, # 38 p. 8259 - 8276