1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C 2: methanol; N-bromosuccinmide / Reflux 3: 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride 4: potassium carbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / Reflux 5: Reflux View Scheme

oxalic acid

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&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=20&deg;C;&nbsp;3&nbsp;h;&nbsp;&nbsp;Inert atmosphere;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3647881', constants.ctx, '0')">sodium</a> <br /> <br /> &nbsp;

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />10&nbsp;h;&nbsp;&nbsp;Reflux;&nbsp;<br /> &nbsp;