2-氯-2-苯基苯乙酮合成路线 (共 108 条)
参考文献
Donnici, Claudio Luis; Guimaraes, Sibele; De Melo, Angelita Cristine
Synthetic Communications, 2003 , vol. 33, # 9 p. 1489 - 1497
反应条件
1: With tributyl-amine; titanium tetrachloride in dichloromethane T=-78°C; 0.5 h; 2: With 2-(diethylcarboxamido)-3-(p-chlorophenyl)oxaziridine in dichloromethane T=-78 - 20°C; 2.5 h;
参考文献
Armstrong, Alan; Edmonds, Ian D.; Swarbrick, Martin E.; Treweeke, Nigel R.
Tetrahedron, 2005 , vol. 61, # 35 p. 8423 - 8442
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78 - 20°C;
参考文献
Brewer, Matthias
Tetrahedron Letters, 2006 , vol. 47, # 44 p. 7731 - 7733
反应条件
boron trifluoride diethyl etherate; water in 1,4-dioxane T=70°C; 10 h;
参考文献
Dement'eva, L. P.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 117 - 118
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 138 - 139
反应条件
1: With allylsamarium bromide in tetrahydrofuran T=20°C; 0.166667 h; 2: With N,N-dimethyl-formamide in tetrahydrofuran T=20°C; 10 h;
参考文献
Di, Jucai; Zhang, Songlin
Synlett, 2008 , # 10 p. 1491 - 1494
反应条件
sodium hypochlorite; water in dichloromethane T=20°C; 4 h;
参考文献
Ruan, Libo; Shi, Min; Li, Nian; Ding, Xu; Yang, Fan; Tang, Jie
Organic Letters, 2014 , vol. 16, # 3 p. 733 - 735
反应条件
1: allyl bromide With samarium in tetrahydrofuran T=20°C; 1.08333 h; Inert atmosphere; 2: α-bromo-α-chloro-deoxybenzoin With N,N-dimethyl-formamide in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Liu, Xiaodan; Zhang, Songlin; Di, Jucai
Synthesis, 2009 , # 16 p. 2749 - 2755
反应条件
chromium(VI) oxide; chloro-trimethyl-silane in tetrachloromethane 20 h; 5-10 degC to room temp.;
参考文献
Lee, Jong Gun; Ha, Dong Soo
Tetrahedron Letters, 1989 , vol. 30, # 2 p. 193 - 196
反应条件
Manganese (II) acetate; acetic anhydride in acetic acid 3 h; Heating;
参考文献
Yonemura, Hiroshi; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3153 - 3160
反应条件
pyridinium chlorochromate in dichloromethane 6 h; Ambient temperature;
参考文献
Wilson, R. Marshall; Chow, Tahsin J.
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4635 - 4636