Bhandari, Prabha; Crombie, Leslie; Daniels, Peter; Holden, Ian; Bruggen, Nicholas Van; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 839 - 850
hydrogen; palladium on activated charcoal in acetone
1 h; Ambient temperature;
参考文献
Bhandari, Prabha; Crombie, Leslie; Daniels, Peter; Holden, Ian; Bruggen, Nicholas Van; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 839 - 850
1: 1.) NaOEt / 1.) EtOH, 2.) reflux, 2 h
2: 100 percent / NaBH4 / H2O; ethanol / 1 h / 20 - 25 °C
3: 97 percent / SOCl2, pyridine / diethyl ether / 0.5 h / below 5 deg C
4: 92 percent / KI, urea / acetone / 6 h / Heating
5: H2 / 10percent Pd/C / acetone / 1 h / Ambient temperature
View Scheme
参考文献
Bhandari, Prabha; Crombie, Leslie; Daniels, Peter; Holden, Ian; Bruggen, Nicholas Van; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 839 - 850
