反应条件
1: 92 percent / 30percent HBr/AcOH / 1 h / Heating
2: 1.) NaH / 1.) THF, RT, 30 min, 2.) THF, RT, 2 h
3: 85percent aq. KOH / 16 h / Heating
4: 3 h / 100 - 180 °C
View Scheme
参考文献
Yamagiwa, Yoshiro; Koreishi, Yoshiro; Kiyozumi, Satoshi; Kobayashi, Masanori; Kamikawa, Tadao; Tsukino, Mitsuji; Goi, Hironori; Yamamoto, Mikiko; Munakata, Megumu
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 11 p. 3317 - 3323
