glass or DBU or Cs2CO3 in tetrahydrofuran; water Kinetics; hydrolysis at 55°C in THF/H2O in the presence of glass powder or DBU or Cs2CO3; not isolated;
参考文献
Lennox, Alastair J. J.; Lloyd-Jones, Guy C.
Journal of the American Chemical Society, 2012 , vol. 134, # 17 p. 7431 - 7441
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2,2'-azo-bisisobutyronitrile react. at 0 °C, then warming to 20 °C, 20 h stirring at 80 °C; saponification of intermediate dibromide;
参考文献
Gmelin Handbook: B: B-Verb.9, 5.3.3, page 238 - 244
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Hoffmann, A. K.; Groszos, St. J.
Patent: US2882317 , 1959 ;
C.A., 1959 , p. 16062