反应条件
1: With N,N,N',N,-tetramethylethylenediamine; tert.-butyl lithium in diethyl ether; pentane
T=-45 - 0°C; 4.25 h; Inert atmosphere;
2: With 1,2-dibromo-1,1,2,2-tetrachloroethane in tetrahydrofuran; diethyl ether; pentane
T=20°C; 17 h; Inert atmosphere; enantioselective reaction;
参考文献
Loelsberg, Wibke; Werle, Susen; Neudoerfl, Joerg-Martin; Schmalz, Hans-Guenther
Organic Letters, 2012 , vol. 14, # 23 p. 5996 - 5999
