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1: 1.) potassium carbonate, 2.) Amberlite IR-120B / 1.) acetone, methanol, rt, 3 h; 2.) 20 h 2: 60 percent / borane-methyl sulfide / tetrahydrofuran / 1.) 0 deg C, 3 h; 2.) rt, 3 h View Scheme

Amberlite IR-120B; potassium carbonate 1.) acetone, methanol, rt, 3 h; 2.) 20 h; Yield given. Multistep reaction;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587194', constants.ctx, '0')">iodine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />2&nbsp;h;&nbsp;&nbsp;Ambient temperature;&nbsp;<br /> &nbsp;