iodobenzene in N,N-dimethyl-formamide
T=5 - 10°C; electrolysis: undivided electrochemical cell, Bu4NBF4 as a supporting electrolyte, sacrificial Mg anode, Ni grid cathode freshly coated with a small deposit of Cd, constant current with density of 1 A dm-2;
zinc in pyridine
T=20°C; P=1500.1 - 3000.2 Torr; 4 h;
参考文献
Tordeux, Marc; Francese, Catherine; Wakselman, Claude
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 7 p. 1951 - 1957