1,5-二溴-3-甲基戊烷合成路线 （共 17 条）
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane T=0°C; 1 h;
参考文献
Mladkova, Jana; Vanek, Vaclav; Budesinsky, Milos; Elbert, Tomas; Demianova, Zuzana; Garrow, Timothy A.; Jiracek, Jiri
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6822 - 6831
反应条件
(i) LiAlH4, (ii) aq. HBr, H2SO4; Multistep reaction;
参考文献
Whitehead et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3632
反应条件
sulfuric acid; hydrogen bromide 3 h; Heating;
参考文献
Odinokov, V. N.; Ishmuratov, G. Yu.; Kharisov, R. Ya.; Yakovleva, M. P.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1991 , vol. 27, # 3 p. 361 - 363
Khimiya Prirodnykh Soedinenii, 1990 , # 3 p. 417 - 419
反应条件
phosphorus pentabromide Kochen des Reaktionsprodukts mit 40prozentiger HBr;
参考文献
Leonard; Wicks
Journal of the American Chemical Society, 1946 , vol. 68, p. 2402
反应条件
1: 44 percent / LiAlH4 / tetrahydrofuran / 2 h / 20 °C 2: 73 percent / PBr3 / 20 h / -10 - 20 °C View Scheme
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
反应条件
hydrogen bromide T=120°C;
参考文献
Wartski,L.
Bulletin de la Societe Chimique de France, 1965 , p. 3066 - 3076
反应条件
bromine; phosphorus tribromide 1.) from 24 deg C to 34 deg C, 2.) reflux, 2 h; Yield given. Multistep reaction;
参考文献
Nguyen, Binh T.; Cartledge, Frank K.
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2206 - 2210
反应条件
1: aqueous sulfuric acid 2: Raney nickel; ethanol / 100 °C / 36775.4 Torr / Hydrogenation 3: water; sulfuric acid; hydrobromic acid View Scheme
参考文献
Ashley et al.
Journal of the Chemical Society, 1958 , p. 3298,3308
反应条件
1: Raney nickel; ethanol / 100 °C / 36775.4 Torr / Hydrogenation 2: water; sulfuric acid; hydrobromic acid View Scheme
参考文献
Ashley et al.
Journal of the Chemical Society, 1958 , p. 3298,3308
反应条件
(i) PBr3, (ii) aq. HBr; Multistep reaction;
参考文献
Volynskii,N.P.; Shcherbakova,L.P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 1006 - 1009
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, # 5 p. 1077 - 1080
