3-甲基-1,5-戊二醇合成路线 (共 33 条)
反应条件
triethylamine; 1,2,3-benzenetriol in benzene
T=50°C; 0.5 h;
参考文献
Stenlake; Waigh; Dewar; et al.
European Journal of Medicinal Chemistry, 1981 , vol. 16, # 6 p. 515 - 524
反应条件
1: PBr3
2: NaNH2 / diethyl ether; liquid ammonia
3: N-ethyl-aniline <Li salt> / diethyl ether
4: aq. HCl / acetic acid
View Scheme
参考文献
Cope,A.C.; Woo,G.L.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3601 - 3608
反应条件
aluminium oxide-chromium oxide; hydrogen sulfide
T=265°C;
参考文献
Hopkins; Rall
A.C.S. Div. Petr. Chim. Preprints, 1957 , vol. 2, # 1 p. 231,236, 239