4-氨基-3-三氟甲基苯酚合成路线 （共 7 条）
反应条件
10 palladium on activated charcoal P=760.051 Torr;
参考文献
Boros, Eric E.; Kaldor, Istvan; Turnbull, Philip S.
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 3 p. 733 - 736
反应条件
1: 1.) NaNO, HCl, Na2CO3, 2.) NaOH / 1.) H2O, 30 min, 2.) H2O, 0-5 deg C 2: 47.2 g / Na2S2O4 / H2O View Scheme
参考文献
Whalley
Journal of the Chemical Society, 1949 , p. 3016,3019
反应条件
sodium dithionite; ethanol
参考文献
Whalley
Journal of the Chemical Society, 1949 , p. 3016,3019
反应条件
1: aqueous H2SO4; NaNO2 / Eintragen der erhaltenen Diazoniumsalz-Loesung in siedende wss. CuSO4-Loesung 2: tin; concentrated aqueous hydrochloric acid View Scheme
参考文献
Whalley
Journal of the Chemical Society, 1949 , p. 3016,3019
反应条件
1: aqueous HCl / Diazotization.Eintragen der Diazoniumsalz-Loesung in siedende wss. CuSO4-Loesung 3: sodium dithionite; aqueous ethanol View Scheme
参考文献
Whalley
Journal of the Chemical Society, 1949 , p. 3016,3019
反应条件
acetic anhydride; acetic acid
T=20°C; 1 h;
参考文献
ORION CORPORATION
Patent: WO2005/794 A1, 2005 ;
Location in patent: Page 31 ;
WO 2005/000794 A1
反应条件
manganese(IV) oxide in sulfuric acid
T=5°C; 2 h;
参考文献
Dieks, Henrik; Senge, Mathias O.; Kirste, Burkhard; Kurreck, Harry
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8666 - 8680
