[1,1'-联苯]-3,4-二甲酸合成路线 （共 17 条）
参考文献
Galanin; Kudrik; Shaposhnikov
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 4 p. 603 - 606
反应条件
1: acetic acid anhydride 2: AlCl3 / 80 °C / Erhitzen des Reaktionsprodukts mit ZnCl2 auf 230grad View Scheme
参考文献
Butterworth et al.
Journal of the Chemical Society, 1938 , p. 1386,1389
反应条件
oxygen; anhydrous cobalt diacetate; sodium bromide in acetic acid
T=95°C; 2 h;
参考文献
Koshel', G. N.; Krestinina, T. B.; Shapiro, Yu. E.; Shutova, I. V.; Ogil'ko, M. N.; et al.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1350 - 1354
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1499 - 1504
反应条件
oxygen; anhydrous cobalt diacetate; sodium bromide in acetic acid
3 h; in a closed system at atmosferic pressure;
参考文献
Koshel', G. N.; Krestinina, T. B.; Shapiro, Yu. E.; Shutova, I. V.; Ogil'ko, M. N.; et al.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1350 - 1354
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1499 - 1504
反应条件
1: 1)H2SO4 / 2)Pd catalyst, KPG (TU 0-02-974-74) / 1) 5-8 deg C, 2 h, 2) 280-320 deg C, 5-6 h
2: 54 percent / cobalt acetate, NaBr, O2 / acetic acid / 4 h / 95 °C
3: 98 percent / cobalt acetate, NaBr, O2 / acetic acid / 2 h / 95 °C
View Scheme
参考文献
Koshel', G. N.; Krestinina, T. B.; Shapiro, Yu. E.; Shutova, I. V.; Ogil'ko, M. N.; et al.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1350 - 1354
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1499 - 1504
反应条件
pyridine; potassium permanganate
参考文献
Newman,M.S.; Eberwein,J.A.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2516 - 2519
反应条件
1: isoamyl nitrite / 48 h / Heating
2: KMnO4
View Scheme
参考文献
Gavina, Francisco; Costero, Ana M.; Gonzalez, Ana M.
Journal of Organic Chemistry, 1990 , vol. 55, # 7 p. 2060 - 2063
反应条件
1: isoamyl nitrite / 48 h / Heating
2: KMnO4
View Scheme
参考文献
Gavina, Francisco; Costero, Ana M.; Gonzalez, Ana M.
Journal of Organic Chemistry, 1990 , vol. 55, # 7 p. 2060 - 2063
反应条件
1: 2.) DDQ / 2.) chlorobenzene
2: alkaline hydrolysis
View Scheme
参考文献
Bapat, Jayant B.; Brown, Roger F.C.; Bulmer, Glenn H.; Childs, Trevor; Coulston, Karen J.; Eastwood, Frank W.; Taylor, Dennis K.
Australian Journal of Chemistry, 1997 , vol. 50, # 12 p. 1159 - 1182
反应条件
1: copper-powder; quinoline
2: water; potassium permanganate; magnesium sulfate
View Scheme
参考文献
Ghigi
Chemische Berichte, 1937 , vol. 70, p. 2469,2472, 2477
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1937 , vol. <6> 26, p. 346,350
