二苯并[c,e]氧杂卓-5(7H)-酮合成路线 (共 16 条)
反应条件
(i) BBr3, (ii) /BRN= 1098229/, H2SO4; Multistep reaction;
参考文献
Kobayashi; Kihara; Mineo
Chemical and Pharmaceutical Bulletin, 1978 , vol. 26, # 2 p. 635 - 639
参考文献
Nose, Atsuko; Kudo, Tadahiro
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 10 p. 4335 - 4339
反应条件
[Cp*Ir(6,6’-(OH)2bpy)(H2O)][OTf]2 in water
6 h; Inert atmosphereRefluxGreen chemistry;
参考文献
Fujita, Ken-Ichi; Ito, Wataru; Yamaguchi, Ryohei
ChemCatChem, 2014 , vol. 6, # 1 p. 109 - 112
反应条件
carbonylchlorohydridetris(triphenylphosphine) ruthenium(II) in toluene
T=110°C; 5 h; Inert atmosphere;
参考文献
Omura, Sohei; Fukuyama, Takahide; Murakami, Yuji; Okamoto, Hiromi; Ryu, Ilhyong
Chemical Communications, 2009 , # 44 p. 6741 - 6743
反应条件
Oxonereg;; 2-iodo-3,4,5,6-tetramethylbenzoic acid in water; acetonitrile
T=30°C; 4 h; Green chemistry;
参考文献
Jhulki, Samik; Seth, Saona; Mondal, Manas; Moorthy, Jarugu Narasimha
Tetrahedron, 2014 , vol. 70, # 13 p. 2286 - 2293
反应条件
Oxonereg;; osmium(VIII) oxide in N,N-dimethyl-formamide
T=20°C; 0.75 h;
参考文献
Schomaker, Jennifer M.; Travis, Benjamin R.; Borhan, Babak
Organic Letters, 2003 , vol. 5, # 17 p. 3089 - 3092
反应条件
sodium tetrahydroborate in N,N-dimethyl-formamide
1 h; Ambient temperature;
参考文献
Brandmeier, Volker; Feigel, Martin
Tetrahedron, 1989 , vol. 45, # 5 p. 1365 - 1376
反应条件
Oxonereg;; osmium(III) chloride in N,N-dimethyl-formamide
T=20°C; 12 h; Product distribution; Further Variations:Catalysts;
参考文献
Whitehead, Daniel C.; Travis, Benjamin R.; Borhan, Babak
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3797 - 3800
反应条件
sodium tetrahydroborate; boron trifluoride diethyl etherate in tetrahydrofuran
参考文献
Sindelar, Karel; Holubek, Jiri; Ryska, Miroslav; Koruna, Ivan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 12 p. 2848 - 2868
反应条件
samarium diiodide; water in tetrahydrofuran
1.25 h; Ambient temperature;
参考文献
Kamochi, Yasuko; Kudo, Tadahiro
Chemistry Letters, 1993 , # 9 p. 1495 - 1498