苯-1,2,3,4,5,6-六胺合成路线 （共 7 条）
反应条件
ammonia; sodium in methanol
Heating;
参考文献
Rogers, Donald Z.
Journal of Organic Chemistry, 1986 , vol. 51, # 20 p. 3904 - 3905
反应条件
hydrogenchloride; tin in 1,4-dioxane
6 h; Heating;
参考文献
Mataka; Eguchi; Takahashi; Hatta; Tashiro
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3127 - 3131
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Praefcke, Klaus; Kohne, Bernd; Korinth, Frank; Psaras, Panicos; Nasielski, Jaques; et al.
Liebigs Annalen der Chemie, 1989 , p. 617 - 622
反应条件
1: 99 percent / NH3-gas / toluene / 10 h / Heating
2: 68 percent / Ph-NH-NH2 / 1.) 120 degC, 2.5 h; 2.) to 140 degC in 2.5 h; 3.) 140 degC, 1h
View Scheme
参考文献
Kohne, Bernd; Praefcke, Klaus
Liebigs Annalen der Chemie, 1985 , # 3 p. 522 - 528
反应条件
1: sulfuric acid; sulfur trioxide; potassium nitrate
2: ammonia / toluene / Heating
3: methanol; ammonia; sodium / Cooling
View Scheme
参考文献
Juarez, Rafael; Ramos, Mar; Segura, Jose L.; Orduna, Jesus; Villacampa, Belen; Alicante, Raquel
Journal of Organic Chemistry, 2010 , vol. 75, # 22 p. 7542 - 7549
参考文献
Fluerscheim; Holmes
Journal of the Chemical Society, 1929 , p. 336
参考文献
Juarez, Rafael; Ramos, Mar; Segura, Jose L.; Orduna, Jesus; Villacampa, Belen; Alicante, Raquel
Journal of Organic Chemistry, 2010 , vol. 75, # 22 p. 7542 - 7549
