反应条件
in hexane
exclusion of moisture, Schlenk technique; addn. of a soln. of borane in hexane to a soln. of arsole in hexane (stirred, 5 min), 2 h (monitored by (11)B NMR); concn., cooled (-78°C), pptn., mixt. of both products, detected by NMR;
参考文献
Brandl, Andreas; Noeth, Heinrich
Chemische Berichte, 1990 , vol. 123, p. 53 - 62
