1-氯-2,4,6-三(三氟甲基)苯合成路线 （共 5 条）
反应条件
n-butyllithium; chlorine in diethyl ether; hexane
参考文献
Carr, G. E.; Chambers, R. D.; Holmes, T. F.; Parker, P. G.
Journal of Organometallic Chemistry, 1987 , vol. 325, p. 13 - 24
反应条件
hydrogen fluoride
T=220 - 280°C;
参考文献
McBee; Leech
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 393
反应条件
1: 33 percent / SF4 / 6 h / 150 °C
2: 66 percent / 1.6 M n-BuLi, Cl2 / diethyl ether; hexane
View Scheme
参考文献
Carr, G. E.; Chambers, R. D.; Holmes, T. F.; Parker, P. G.
Journal of Organometallic Chemistry, 1987 , vol. 325, p. 13 - 24
反应条件
1: tetrachloromethane; chlorine / 80 °C / Irradiation
2: HF / 220 - 280 °C
View Scheme
参考文献
McBee; Leech
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 393
参考文献
McBee; Leech
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 393
