1-碘-2,4,6-三硝基苯合成路线 （共 13 条）
反应条件
in tetrahydrofuran byproducts: 1,3,5-trinitrobenzene; vac., 50°C, 96 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 2 p. 432
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 476 - 477
参考文献
Hepp
Justus Liebigs Annalen der Chemie, 1882 , vol. 215, p. 363
Bulletin de la Societe Chimique de France, 1878 , vol. <2>30, p. 5
反应条件
potassium trimethylstannate in tetrahydrofuran T=0 - 5°C;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 3 p. 640
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 715 - 716
反应条件
hydrogen iodide; acetone
参考文献
Meyer,J.
Patent: DE234726 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 122
反应条件
in tetrahydrofuran 72 h; Yields of byproduct given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 1649 - 1659
Zhurnal Organicheskoi Khimii, , vol. 20, # 8 p. 1809 - 1820
反应条件
(Ph3P)2Pd(Ph)(I) in 1,2-dichloro-ethane T=120 - 130°C; 1.5 h;
参考文献
Kashin, N. A.; Bumagina, I. G.; Bumagin, N. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 1 p. 18 - 24
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 21 - 28
反应条件
tetra-(n-butyl)ammonium iodide; (Ph3P)2Pd(Ph)(I) in tetrahydrofuran T=64°C; 1 h;
参考文献
Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 10 p. 1993
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 10 p. 2413 - 2414
反应条件
sodium hydroxide in water T=25°C; Rate constantMechanismEquilibrium constant;
参考文献
Crampton, Michael R.; Davis, Antony B.; Greenhalgh, Colin; Stevens, J. Andrew
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 675 - 682
反应条件
sodium iodide in acetic acid; acetone
T=25°C; 0.5 h;
参考文献
Boiko, V. N.; Kirii, N. V.; Yagupolskii, L. M.
Journal of Fluorine Chemistry, 1994 , vol. 67, # 2 p. 119 - 124
反应条件
hydrogen iodide in benzene
T=25°C; 0.666667 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nielsen, Arnold T.; Chafin, Andrew P.; Christian, Stephen L.
Journal of Organic Chemistry, 1984 , vol. 49, # 24 p. 4575 - 4580
