双(2-甲氧基乙氧基)甲烷合成路线 (共 7 条)
反应条件
iron(III) chloride bei langsamer Destillation;
参考文献
Sokolowski,A.; Burczyk,B.
Polish Journal of Chemistry, 1979 , vol. 53, p. 905 - 912
反应条件
tetrabutylammomium bromide in benzene T=75°C; 5 h; effect of temperature, various catalysts, various dihalomethanes, further alcohols; Product distribution;
参考文献
Nazaretyan; Torosyan; Babayan
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 11 pt 2 p. 2396 - 2400
反应条件
sodium iodide 1.) acetone, reflux, overnight, 2.) 110 deg C, 0.05 mmHg; Multistep reaction. Title compound not separated from byproducts;
参考文献
Horley, Graeme A.; Ozturk, Turan; Turksoy, Figen; Wallis, John D.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 19 p. 3225 - 3231
反应条件
4 h; Ambient temperature;
参考文献
Nikolic, Nikola A.; Gonda, Elizabeth; Longford, C. P. Desmond; Lane, Nancy T.; Thompson, David W.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2748 - 2751
参考文献
Celanese Corp.
Patent: US2331367 , 1941 ;
参考文献
Saurefabrik Schweizerhall
Patent: US5637775 A1, 1997 ;
反应条件
titanium tetrachloride in dichloromethane T=0°C; 1 h;
参考文献
Nikolic, Nikola A.; Gonda, Elizabeth; Longford, C. P. Desmond; Lane, Nancy T.; Thompson, David W.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2748 - 2751