5H-二茚并[1,2-a:1',2'-c]芴-5,10,15-三酮合成路线 (共 49 条)
反应条件
hydrazine hydrate in diethylene glycol T=180°C; Wolff-Kishner Reduction; 24 h; Temperature;
参考文献
Oded, Yaacov Netanel; Agranat, Israel
Tetrahedron Letters, 2014 , vol. 55, # 3 p. 636 - 638
参考文献
Kimura, Makoto; Kuwano, Seiichi; Sawaki, Yasuhiko; Fujikawa, Hisayoshi; Noda, Koji; Taga, Yasunori; Takagi, Katsuhiko
Journal of Materials Chemistry, 2005 , vol. 15, # 24 p. 2393 - 2398
反应条件
air; graphene-supported KOH composite in N,N-dimethyl-formamide
T=20°C; 36 h;
参考文献
Zhang, Xin; Ji, Xuan; Su, Ruifei; Weeks, Brandon L.; Zhang, Zhao; Deng, Songlu
ChemPlusChem, 2013 , vol. 78, # 7 p. 703 - 711
反应条件
lithium perchlorate; triethylamine
T=120°C; 0.416667 h; Microwave irradiation; chemoselective reaction;
参考文献
Sharma, Lalit Kumar; Kim, Kyung Bo; Elliott, Gregory I.
Green Chemistry, 2011 , vol. 13, # 6 p. 1546 - 1549
反应条件
piperidine; pyridine
参考文献
Ionescu
Chemische Berichte, 1927 , vol. 60, p. 1232
反应条件
pyridinium chlorochromate in dichloromethane
4 h; Ambient temperature;
参考文献
Plater, M. John; Praveen, Marapaka
Tetrahedron Letters, 1997 , vol. 38, # 6 p. 1081 - 1082
反应条件
copper(II) oxide in quinoline
参考文献
Anastassiou,A.G.; Griffin,G.W.
Journal of Organic Chemistry, 1968 , vol. 33, # 9 p. 3441 - 3448
反应条件
1: 72 percent / 6 eq N-bromosuccinimide (NBS), azobisisobutyronitrile (AIBN) / CCl4 / 3 h / Heating
2: 20 percent / conc. H2SO4 / tetrahydrofuran / 5 h / Heating
3: 32 percent / PCC / CH2Cl2 / 4 h / Ambient temperature
View Scheme
参考文献
Plater, M. John; Praveen, Marapaka
Tetrahedron Letters, 1997 , vol. 38, # 6 p. 1081 - 1082
反应条件
1: 20 percent / conc. H2SO4 / tetrahydrofuran / 5 h / Heating
2: 32 percent / PCC / CH2Cl2 / 4 h / Ambient temperature
View Scheme
参考文献
Plater, M. John; Praveen, Marapaka
Tetrahedron Letters, 1997 , vol. 38, # 6 p. 1081 - 1082
反应条件
1: 43 percent / HC(OMe)3, HCl / ethanol / 24 h / Ambient temperature
2: 72 percent / 6 eq N-bromosuccinimide (NBS), azobisisobutyronitrile (AIBN) / CCl4 / 3 h / Heating
3: 20 percent / conc. H2SO4 / tetrahydrofuran / 5 h / Heating
4: 32 percent / PCC / CH2Cl2 / 4 h / Ambient temperature
View Scheme
参考文献
Plater, M. John; Praveen, Marapaka
Tetrahedron Letters, 1997 , vol. 38, # 6 p. 1081 - 1082