2-异硫代苯并二氢吡喃-4-酮合成路线 (共 13 条)
反应条件
quinolinium monofluorochromate(VI) in acetonitrile Oxidation; 5 h; Heating;
参考文献
Bose, D. Subhas; Reddy, A. V. Narsimha; Das, A. P. Rudra
Synthesis, 2003 , # 12 p. 1883 - 1885
反应条件
aluminium trichloride in carbon disulfide 3 h; Ambient temperature;
参考文献
Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; El-Zohry, Maher F.; Khalaf, Ali A.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 31 - 44
反应条件
kieselguhr; phosphorus pentoxide; benzene
参考文献
Akkurt; YIldIrIm; Kerbal; Bennani; Hadda, T. Ben; Chohan; McKee, Vickie
Journal of Chemical Crystallography, 2010 , vol. 40, # 2 p. 165 - 168
反应条件
THF-d8 (tetrahydrofuran-d8); selenium(IV) oxide T=26°C; 4 h;
参考文献
Toshima, Kazunobu; Ohta, Kazumi; Ohtake, Tatsuya; Tatsuta, Kuniaki
Journal of the Chemical Society, Chemical Communications, 1991 , # 10 p. 694 - 695
反应条件
tetrachloromethane; selenium(IV) oxide; oxygen T=26°C; 42 h;
参考文献
Toshima, Kazunobu; Ohta, Kazumi; Ohtake, Tatsuya; Tatsuta, Kuniaki
Journal of the Chemical Society, Chemical Communications, 1991 , # 10 p. 694 - 695
反应条件
selenium(IV) oxide in 1,4-dioxane; water
参考文献
Toshima, Kazunobu; Ohta, Kazumi; Ohtake, Tatsuya; Tatsuta, Kuniaki
Journal of the Chemical Society, Chemical Communications, 1991 , # 10 p. 694 - 695
反应条件
1: hydrogenchloride; acetic acid / water 2: thionyl chloride 3: AlCl3, aluminium chloride View Scheme
参考文献
Akkurt; YIldIrIm; Kerbal; Bennani; Hadda, T. Ben; Chohan; McKee, Vickie
Journal of Chemical Crystallography, 2010 , vol. 40, # 2 p. 165 - 168
反应条件
1: ethanol; water 2: hydrogenchloride; acetic acid / water 3: thionyl chloride 4: AlCl3, aluminium chloride View Scheme
参考文献
Akkurt; YIldIrIm; Kerbal; Bennani; Hadda, T. Ben; Chohan; McKee, Vickie
Journal of Chemical Crystallography, 2010 , vol. 40, # 2 p. 165 - 168
反应条件
1: 1.) conc. HCl / 2.) MeOH 2: 1.) NaOH, 2.) TFA, TFAA / 1.) EtOH View Scheme
参考文献
Bertenshaw, Stephen R.; Talley, John J.; Rogier; Graneto, Matthew J.; Koboldt, Carol M.; Zhang, Yan
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2827 - 2830
反应条件
sodium hydroxide; trifluoroacetic acid; trifluoroacetic anhydride 1.) EtOH; Yield given. Multistep reaction;
参考文献
Bertenshaw, Stephen R.; Talley, John J.; Rogier; Graneto, Matthew J.; Koboldt, Carol M.; Zhang, Yan
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2827 - 2830