2-氯-10H-吩噻嗪-10-丙腈合成路线 （共 8 条）
反应条件
nickel; dimethyl amine; benzene T=110 - 116°C; P=58840.6 Torr; Hydrogenation;
参考文献
Fujii
Yakugaku Zasshi, 1956 , vol. 76, p. 644,647, 648
Chem.Abstr., 1957 , p. 425
反应条件
ethanol; ammonia; nickel T=100 - 110°C; P=66195.7 Torr; Hydrogenation;
参考文献
Godefroi; Wittle
Journal of Organic Chemistry, 1956 , vol. 21, p. 1163,1168
Full Text Show Details
Soc. Usines Chim. Rhone-Poulenc
Patent: DE1012915 , 1957 ;
反应条件
nickel; dimethyl amine; benzene T=110 - 116°C; P=58840.6 Torr; Hydrogenation;
参考文献
Fujii
Yakugaku Zasshi, 1956 , vol. 76, p. 644,647, 648
Chem.Abstr., 1957 , p. 425
反应条件
1: Raney nickel; benzene / 100 - 105 °C / 36775.4 Torr 2: LiAlH4; diethyl ether; dioxane View Scheme
参考文献
Fujii
Yakugaku Zasshi, 1956 , vol. 76, p. 644,647, 648
Chem.Abstr., 1957 , p. 425
反应条件
N-benzyl-trimethylammonium hydroxide in 1,4-dioxane
90 h;
参考文献
Brufani; Cesta; Filocamo; Lappa; Marta; Pomponi; Meroni; Pagella
Farmaco, 1992 , vol. 47, # 5 p. 585 - 597
反应条件
1: iodine; sulfur
2: hydroquinone; tri-N-methyl-anilinium hydroxide
View Scheme
参考文献
Sawizkaja et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 2900,2903; engl. Ausg. S. 3227, 3229
反应条件
sodium hydroxide; water in methanol
16 h; Heating;
参考文献
Brufani; Cesta; Filocamo; Lappa; Marta; Pomponi; Meroni; Pagella
Farmaco, 1992 , vol. 47, # 5 p. 585 - 597
反应条件
1: Raney nickel; dioxane / 108 - 116 °C / 33097.9 Torr / Hydrogenation.Behandeln des Reaktionsprodukts mit wss. Ameisensaeure und wss. Formaldehyd
2: CH3I; aq.-ethanolic NaOH
View Scheme
参考文献
Fujii
Yakugaku Zasshi, 1956 , vol. 76, p. 644,647, 648
Chem.Abstr., 1957 , p. 425
