3-(3-甲基-1H-1-吲哚)丙腈合成路线 （共 9 条）
反应条件
potassium hydroxide 3 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 11 p. 1018 - 1022
反应条件
Ni(PPh3)4 in toluene
T=70°C; 5 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rodriguez, J. G.; Canoira, L.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 883 - 888
反应条件
Ni(PPh3)4 in toluene
T=65°C; 5 h;
参考文献
Rodriguez, J. G.; Canoira, L.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 883 - 888
反应条件
n-butyl-magnesium chloride
1.) THF, RT, 1 h, 2.) THF, RT, 24 h; Yield givenMultistep reaction;
参考文献
Rodriguez, J. Gonzalo; Urrutia, Anahi
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 1 p. 129 - 135
反应条件
1: 19 percent / Na2CO3 / ethanol; H2O / 52 h / Heating
2: 1.)tetrakis(triphenylphosphine)nickel(0) 2.)2,3-dichloro-5,6-dicyano-p-benzoquinone / 1.)toluene, 65 deg C, 5 h 2.)toluene, reflux, 3 h
View Scheme
参考文献
Rodriguez, J. G.; Canoira, L.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 883 - 888
反应条件
in ethanol
24 h; Heating;
参考文献
Basanagoudar, L D; Mahajanshetti, C S; Dambal, S B
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 11 p. 1018 - 1022
反应条件
Ni(PPh3)4; 2,3-dicyano-5,6-dichloro-p-benzoquinone
1.)toluene, 65 deg C, 5 h 2.)toluene, reflux, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rodriguez, J. G.; Canoira, L.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 883 - 888
反应条件
in methanol
9 h; Irradiation; Further byproducts given;
参考文献
Donati, Donato; Fusi, Stefania; Ponticelli, Fabio; Roncucci, Gabrio
Gazzetta Chimica Italiana, 1994 , vol. 124, # 2 p. 71 - 76
反应条件
hydrogen; nickel in methanol
P=3102.9 Torr; 6 h;
参考文献
Basanagoudar, L D; Mahajanshetti, C S; Dambal, S B
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 11 p. 1018 - 1022
