4-戊烯-1-基 6-O-[(2-甲基-2-丙基)(二苯基)硅烷基]-D-吡喃葡萄糖苷合成路线 (共 4 条)
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine 12 h; Ambient temperature;
参考文献
Ratcliffe; Konradsson; Reid
Carbohydrate Research, 1991 , vol. 216, p. 323 - 335
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
22 h;
参考文献
Ruttens, Bart; Van Der Eycken, Johan
Tetrahedron Letters, 2002 , vol. 43, # 12 p. 2215 - 2221
反应条件
1: 85 percent / PTSA / CHCl3 / 70 h / 90 °C
2: 94 percent / DBU / tetrahydrofuran / 22 h
View Scheme
参考文献
Ruttens, Bart; Van Der Eycken, Johan
Tetrahedron Letters, 2002 , vol. 43, # 12 p. 2215 - 2221
反应条件
1: 85 percent / PTSA / CHCl3 / 70 h / 90 °C
2: 94 percent / DBU / tetrahydrofuran / 22 h
View Scheme
参考文献
Ruttens, Bart; Van Der Eycken, Johan
Tetrahedron Letters, 2002 , vol. 43, # 12 p. 2215 - 2221