2-苯二(甲)酰亚氨基乙烷磺酰氯合成路线 (共 8 条)
反应条件
phosphorus pentachloride; potassium acetate in water; acetic acid; toluene
参考文献
Pfizer INC
Patent: US6313312 B1, 2001 ;
反应条件
phosphorus pentachloride in benzene
参考文献
Shin, Kye Jung; Yoo, Kyung Ho; Kim, Dong Jin; Park, Sang Woo; Ko, Bong Suck; Lee, Sang Joo; Huh, Jae Doo; Park, Seung Yong
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 13 p. 1607 - 1612
反应条件
thionyl chloride; N,N-dimethyl-formamide 5 h; Heating;
参考文献
Humljan, Jan; Gobec, Stanislav
Tetrahedron Letters, 2005 , vol. 46, # 23 p. 4069 - 4072
Title/Abstract Full Text View citing articles Show Details
Humljan, Jan; Kotnik, Miha; Boniface, Audrey; Solmajer, Tomaz; Urleb, Uros; Blanot, Didier; Gobec, Stanislav
Tetrahedron, 2006 , vol. 62, # 47 p. 10980 - 10988
反应条件
hydrogenchloride; N-chloro-succinimide in water; acetonitrile T=10 - 20°C; 0.5 h; Green chemistry;
参考文献
Yang, Zhanhui; Xu, Jiaxi
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-H0216-OP, p. 1675 - 1682
反应条件
1: 90 percent / CH3COOK, AcOH 2: 85 percent / PCl5 / benzene View Scheme
参考文献
Yudakhina; Moreva; Zarubin; Purygin
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 6 p. 934 - 935
Zh. Org. Khim., 2013 , vol. 49, # 6 p. 947 - 948,2
反应条件
methanol; zinc Erhitzen des Reaktionsprodukts mit wss.NaOH;
参考文献
Pichat; Herbert
Bulletin de la Societe Chimique de France, 1958 , p. 820
参考文献
PARADIGM THERAPEUTICS LTD.
Patent: WO2007/582 A1, 2007 ;
Location in patent: Page/Page column 39; 88 ;
WO 2007/000582 A1
反应条件
ammonia in dichloromethane
T=0 - 20°C;
参考文献
Usifoh, Cyril O.; Lambert, Didier M.; Wouters, Johan; Scriba, Gerhard K.E.
Archiv der Pharmazie, 2001 , vol. 334, # 10 p. 323 - 331