(3-氨丙基)磷酸二乙酯合成路线 （共 14 条）
反应条件
hydrogenchloride 18 h; Heating;
参考文献
Fabre, Genevieve; Collignon, Noel; Savignac, Philippe
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2864 - 2869
反应条件
hydrogenchloride 15 h; Heating;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 10, p. 81 - 86
反应条件
1: With sodium tetrahydroborate; cobalt(II) chloride in methanol
T=-30 - 20°C;
2: With hydrogenchloride in water
3: With ammonia in water
pH=9;
参考文献
UNIVERSITY OF VIRGINIA PATENT FOUNDATION
Patent: WO2005/115150 A2, 2005 ;
Location in patent: Page/Page column 89 ;
WO 2005/115150 A2
反应条件
hydrogen; palladium over charcoal in methanol
P=2068.65 Torr; 3 h;
参考文献
Gelder, Joel M. Van; Klein, Joseph Y.; Basel, Yochai; Reizelman, Anat; Tchilibon, Susanna; Mouallem, Orly
Patent: US2008/39456 A1, 2008 ;
Location in patent: Page/Page column 52 ;
反应条件
hydrazine in ethanol
T=20°C; Ring cleavage; 12 h;
参考文献
Gali, Hariprasad; Prabhu, Kandikere R.; Karra, Srinivasa R.; Katti, Kattesh V.
Journal of Organic Chemistry, 2000 , vol. 65, # 3 p. 676 - 680
反应条件
hydrogen; palladium on activated charcoal in ethanol
T=55°C; 17 h;
参考文献
Fabre, Genevieve; Collignon, Noel; Savignac, Philippe
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2864 - 2869
反应条件
ammonium acetate; sodium cyanoborohydride in methanol
T=25°C; 6 h;
参考文献
Collignon, N.; Fabre, G.; Varlet, J. M.; Savignac, Ph.
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 10, p. 81 - 86
反应条件
1: 93 percent / dimethylformamide / 8 h / 100 °C
2: 51 percent / H2NNH2*H2O / ethanol / 1 h / Heating
View Scheme
参考文献
Bako, Peter; Novak, Tibor; Ludanyi, Krisztina; Pete, Bela; Toke, Laszlo; Keglevich, Gyoergy
Tetrahedron Asymmetry, 1999 , vol. 10, # 12 p. 2373 - 2380
参考文献
Verbruggen, Christophe; De Craecker, Sofie; Rajan, Padinchare; Jiao, Xian-Yun; Borloo, Marianne; Smith, Keith; Fairlamb, Alan H.; Haemers, Achiel
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 3 p. 253 - 258
参考文献
Dynamit Nobel Aktiengesellschaft
Patent: US4029679 A1, 1977 ;
