2-(氯羰基)苯甲酸甲酯合成路线 (共 40 条)
反应条件
aluminium trichloride T=10°C; anschl. Erhitzen auf 80grad;
参考文献
Smith
Journal of the American Chemical Society, 1921 , vol. 43, p. 1920
反应条件
1: pyridine; hydrazine hydrate 2: aq. NaOH solution View Scheme
参考文献
Journal of the Chemical Society, , p. 16,25
反应条件
sulfuric acid; 1,1,1,3,3,3-hexamethyl-disilazane 1.) CH2Cl2, room temp., 2.) CH3OH; Yield given. Multistep reaction;
参考文献
Fisher, Lawrence E.; Caroon, Joan M.; Jahangir; Stabler, S. Russell; Lundberg, Scott; Muchowski, Joseph M.
Journal of Organic Chemistry, 1993 , vol. 58, # 14 p. 3643 - 3647
反应条件
Pd-BaSO4; sulfur; xylene T=180°C; weiteres Reagens: Chinolin;
参考文献
Entwistle, Ian D.; Boehm, Peter; Johnstone, Robert A. W.; Telford, Robert P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 27 - 30
反应条件
in diethyl ether T=-20°C; Yield given;
参考文献
Ishikawa, Masayuki; Eguchi, Yukuo
Heterocycles, 1981 , vol. 16, # 1 p. 25 - 30
反应条件
2: 150 °C View Scheme
参考文献
Stoermer; Steinbeck
Chemische Berichte, 1932 , vol. 65, p. 413,417
反应条件
sodium tetrahydroborate; potassium carbonate in dichloromethane; water T=0 - 15°C; chemoselective reaction;
参考文献
Rajan, Ramya; Badgujar, Sachin; Kaur, Kamaljit; Malpani, Yashwardhan; Kanjilal, Pranab R.
Synthetic Communications, 2010 , vol. 40, # 19 p. 2897 - 2907
反应条件
1: 2 h / Heating 2: 90 percent 3: 66 percent / NaBH4 / tetrahydrofuran / 1) 0 deg C, 2 h, 2) rt, 2 h View Scheme
参考文献
Kasturi; Pragnacharyulu
Tetrahedron, 1992 , vol. 48, # 21 p. 4431 - 4438
参考文献
Meyer,H.
Monatshefte fuer Chemie, 1901 , vol. 22, p. 578
参考文献
Mannich; Schmitt
Archiv der Pharmazie (Weinheim, Germany), 1928 , p. 80
Chem. Zentralbl., 1927 , vol. 98, # I p. 951