(2,4,5-三甲基苯基)甲醇合成路线 （共 20 条）
参考文献
Lake; Corson
Journal of Organic Chemistry, 1959 , vol. 24, p. 1823
反应条件
1: pyridine; benzene; thionyl chloride 2: aqueous Na2CO3 View Scheme
参考文献
Lake; Corson
Journal of Organic Chemistry, 1959 , vol. 24, p. 1823
反应条件
1: With ruthenium in 1,2,4,5-tetramethyl benzene Heating / reflux; 2: With hydrogen in 1,2,4,5-tetramethyl benzene T=150°C; P=9000.9 Torr; 1 h; Product distribution / selectivity;
参考文献
MITSUBISHI GAS CHEMICAL COMPANY, INC.
Patent: US2005/85663 A1, 2005 ;
Location in patent: Page/Page column 4-6 ;
反应条件
1: concentrated aqueous HCl 2: ethanol View Scheme
参考文献
Smith; MacMullen
Journal of the American Chemical Society, 1936 , vol. 58, p. 629,634
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid
T=25°C; P=760 Torr; 3 h;
参考文献
Yoshino, Yasushi; Hayashi, Yoshiaki; Iwahama, Takahiro; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6810 - 6813
反应条件
hydrogen; dimethyl amine; nickel in ethanol
T=200 - 220°C;
参考文献
Arai,A.; Ichikizaki,I.
Bulletin of the Chemical Society of Japan, 1961 , vol. 34, p. 1571 - 1583
反应条件
sulfuric acid; water; oxygen; [Acr+-Mes]ClO4- in acetonitrile
1.33333 h; Irradiation; Quantum yield; Reagent/catalyst;
参考文献
Ohkubo, Kei; Mizushima, Kentaro; Iwata, Ryosuke; Souma, Kazunori; Suzuki, Nobuo; Fukuzumi, Shunichi
Chemical Communications, 2010 , vol. 46, # 4 p. 601 - 603
反应条件
TNM in various solvent(s)
T=20°C; 0.5 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
TNM in various solvent(s)
T=20°C; 2 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
nitrogen(IV) oxide in dichloromethane
T=20°C; 0.5 h; in the dark; Further byproducts given. Title compound not separated from byproducts;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
