2-羟基-1,2-二(2-甲基苯基)乙酮合成路线 (共 5 条)
反应条件
carbon nitride graphitic; oxygen; acetic acid in water; acetonitrile T=100°C; P=2250.23 Torr; 16 h; AutoclaveIrradiationGreen chemistry;
参考文献
Zhan, Haiying; Liu, Wenjie; Fu, Minling; Cen, Jinghe; Lin, Jingxin; Cao, Hua
Applied Catalysis A: General, 2013 , vol. 468, p. 184 - 189
反应条件
IBuMe
T=65°C; Benzoin condensation; 2 h; Ionic liquid;
参考文献
Chiarotto; Feroci; Orsini; Feeney; Inesi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3287 - 3292
反应条件
3-(2,6-diisopropylphenyl)-4,5-dimethylthiazol-3-ium perchlorate; triethylamine in ethanol
T=60°C; Stetter reaction; 22 h; Inert atmosphere; chemoselective reaction;
参考文献
Piel, Isabel; Pawelczyk, Marius D.; Hirano, Keiichi; Froehlich, Roland; Glorius, Frank
European Journal of Organic Chemistry, 2011 , # 28 p. 5475 - 5484
反应条件
1,4-diaza-bicyclo[2.2.2]octane; oxygen; potassium carbonate; zinc oxide in toluene
T=60°C; 18 h;
参考文献
Muthupandi, Pandi; Sekar, Govindasamy
Tetrahedron Letters, 2011 , vol. 52, # 6 p. 692 - 695
反应条件
zinc sulfate heptahydrate powder; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; QNH in toluene
T=60°C; 36 h; Resolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Muthupandi, Pandi; Sekar, Govindasamy
Tetrahedron Asymmetry, 2011 , vol. 22, # 5 p. 512 - 517