2-乙酰基-3-甲基苯甲酸合成路线 (共 5 条)
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane Inert atmosphere;
参考文献
Dean, Melissa A.; Hitchcock, Shawn R.
Tetrahedron Asymmetry, 2010 , vol. 21, # 20 p. 2471 - 2478
参考文献
Wuenschell, Gerald E.; Tetreau, Catherine; Lavalette, Daniel; Reed, Christopher A.
Journal of the American Chemical Society, 1992 , vol. 114, # 9 p. 3346 - 3355
反应条件
phosphorus pentachloride; Petroleum ether
参考文献
Przhiyalgovskaya, N. M.; Kon'kov, L. I.; Kurkovskaya, L. N.; Mandzhikov, V. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 10 p. 1078 - 1081
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 10 p. 1346 - 1349
反应条件
1: CCl4; bromine / Irradiation
2: aqueous Na2CO3
View Scheme
参考文献
Eliel; Rivard
Journal of Organic Chemistry, 1952 , vol. 17, p. 1252,1255
反应条件
1: DCC / tetrahydrofuran / 3 - 5 °C
2: 1.4 g / NaH / tetrahydrofuran / 2.5 h / 20 °C
3: 59 percent / EtONa / ethanol / 24 h / 20 °C
View Scheme
参考文献
Athanasellis, Giorgos; Melagraki, Georgia; Chatzidakis, Haralambos; Afantitis, Antreas; Detsi, Anastasia; Igglessi-Markopoulou, Olga; Markopoulos, John
Synthesis, 2004 , # 11 p. 1775 - 1782