3,5-二甲氧基-4-羟基苯乙酸合成路线 (共 14 条)
反应条件
sodium hydroxide in ethanol; water T=20°C; 6 h;
参考文献
Jung; Kang; Lee; Seong; Ham; Park
Synthetic Communications, 2001 , vol. 31, # 3 p. 455 - 462
反应条件
1: H2O 2: dimethylformamide 3: aq. NaOH View Scheme
参考文献
Short,J.H. et al.
Tetrahedron, 1973 , vol. 29, p. 1931 - 1939
反应条件
1: dimethylformamide 2: aq. NaOH View Scheme
参考文献
Short,J.H. et al.
Tetrahedron, 1973 , vol. 29, p. 1931 - 1939
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / benzene / 7 - 20 °C 2: 4 h / 0 °C 3: water / Photolysis View Scheme
参考文献
Givens, Richard S.; Stensrud, Kenneth; Conrad, Peter G.; Yousef, Abraham L.; Perera, Chamani; Senadheera, Sanjeewa N.; Heger, Dominik; Wirz, Jakob
Canadian Journal of Chemistry, 2011 , vol. 89, # 3 p. 364 - 384
反应条件
1: diazomethane / diethyl ether / -5 - 0 °C 2: ammonium acetate / water; methanol / 8 h / 50 °C 3: water; biphenyl / acetonitrile / 0.13 h / |Irradiation View Scheme
参考文献
Senadheera, Sanjeewa N.; Evans, Anthony S.; Toscano, John P.; Givens, Richard S.
Photochemical and Photobiological Sciences, 2014 , vol. 13, # 2 p. 324 - 341
反应条件
1: thionyl chloride / 8 h / 80 °C / |Inert atmosphere 2: diazomethane / diethyl ether / -5 - 0 °C 3: ammonium acetate / water; methanol / 8 h / 50 °C 4: water; biphenyl / acetonitrile / 0.13 h / |Irradiation View Scheme
参考文献
Senadheera, Sanjeewa N.; Evans, Anthony S.; Toscano, John P.; Givens, Richard S.
Photochemical and Photobiological Sciences, 2014 , vol. 13, # 2 p. 324 - 341
参考文献
Short,J.H. et al.
Tetrahedron, 1973 , vol. 29, p. 1931 - 1939
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Arlt et al.
Tappi, 1958 , vol. 41, p. 64,65
Full Text Show Details
Gorecki; Pepper
Canadian Journal of Chemistry, 1959 , vol. 37, p. 2089,2091
参考文献
Gorecki; Pepper
Canadian Journal of Chemistry, 1959 , vol. 37, p. 2089,2091
反应条件
1: aqueous NaOH 4: aq.-ethanolic KOH View Scheme
参考文献
Gorecki; Pepper
Canadian Journal of Chemistry, 1959 , vol. 37, p. 2089,2091