3-羟基-4-甲氧基苯甲醇合成路线 （共 30 条）
反应条件
potassium tert-butylate in propan-1-ol T=60 - 90°C; 5.5 h; Heating / reflux;
参考文献
EURO-CELTIQUE S.A.
Patent: EP1202628 B1, 2004 ;
Location in patent: Page 11 ;
EP 1202628 B1
反应条件
potassium carbonate in acetone 4 h; RefluxInert atmosphere;
参考文献
Taylor, Laura L.; Goldberg, Frederick W.; Hii, King Kuok Mimi
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 22 p. 4424 - 4432
反应条件
1: acetonitrile / 6 h / Reflux 2: potassium hydroxide / ethanol / 5 h / Reflux; Inert atmosphere View Scheme
参考文献
Guo, Xiaotao; Zhang, Dan; Yu, Zhifang; Liu, Tianzhen; Li, Dachang; Li, Chunbao
Journal of Chemical Research, 2011 , vol. 35, # 4 p. 229 - 230
反应条件
silica gel; Bobbitt's oxidant in dichloromethane
参考文献
Bobbitt, James M.
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9367 - 9374
反应条件
1: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran T=20°C; Darkness; 2: With sodium dithionite; water in tetrahydrofuran Darkness;
参考文献
Pouysegu, Laurent; Sylla, Tahiri; Garnier, Tony; Rojas, Luis B.; Charris, Jaime; Deffieux, Denis; Quideau, Stephane
Tetrahedron, 2010 , vol. 66, # 31 p. 5908 - 5917
反应条件
1: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran T=20°C; Darkness; 2: With sodium dithionite; water in tetrahydrofuran Darkness;
参考文献
Pouysegu, Laurent; Sylla, Tahiri; Garnier, Tony; Rojas, Luis B.; Charris, Jaime; Deffieux, Denis; Quideau, Stephane
Tetrahedron, 2010 , vol. 66, # 31 p. 5908 - 5917
反应条件
1: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran T=20°C; Darkness; 2: With sodium dithionite; water in tetrahydrofuran Darkness;
参考文献
Pouysegu, Laurent; Sylla, Tahiri; Garnier, Tony; Rojas, Luis B.; Charris, Jaime; Deffieux, Denis; Quideau, Stephane
Tetrahedron, 2010 , vol. 66, # 31 p. 5908 - 5917
反应条件
1: sodium methylate; methanol / auf dem Dampfbad 2: SOCl2 / 20 °C View Scheme
参考文献
Bersch
Archiv der Pharmazie (Weinheim, Germany), 1939 , vol. 277, p. 271,281
反应条件
1: potassium carbonate / acetonitrile / 10 h / 25 - 35 °C / Reflux 2: phosphorus tribromide / dichloromethane / 2 h / 0 - 10 °C View Scheme
参考文献
WATSON LABORATORIES, INC.; BHANU, Manjunath, Narayan; NAIK, Samir; THOMAS, Rejoy
Patent: WO2012/78147 A1, 2012 ;
反应条件
potassium carbonate in water; acetone
参考文献
WATSON LABORATORIES, INC.; BHANU, Manjunath, Narayan; NAIK, Samir; THOMAS, Rejoy
Patent: WO2012/78147 A1, 2012 ;
Location in patent: Page/Page column 16-17 ;
