2,4,6-三甲基苯甲酰胺合成路线 （共 44 条）
反应条件
1,2-dibromo-1,1,2,2-tetrachloroethane; triethylamine; triphenylphosphine in 1,2-dichloro-ethane T=0°C; 0.0166667 h;
参考文献
Bringmann, Gerhard; Schneider, Stephan
Synthesis, 1983 , # 2 p. 139 - 141
反应条件
1: With trifluorormethanesulfonic acid
T=60°C; Friedel Crafts acylation; 2 h;
2: With water
Cooling;
参考文献
Naredla, Rajasekhar Reddy; Klumpp, Douglas A.
Tetrahedron Letters, 2012 , vol. 53, # 35 p. 4779 - 4781
反应条件
sulfuric acid; acetic acid
T=90°C; 7 h;
参考文献
Moorthy, Jarugu Narasimha; Singhal, Nidhi
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1926 - 1929
参考文献
Tsai et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 2530
反应条件
lead(IV) acetate; N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran
T=25°C; 4 h;
参考文献
Wegmann, Helmut; Steglich, Wolfgang
Chemische Berichte, 1981 , vol. 114, # 7 p. 2580 - 2594
反应条件
lead(IV) acetate; N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran
T=25°C; 4 h;
参考文献
Wegmann, Helmut; Steglich, Wolfgang
Chemische Berichte, 1981 , vol. 114, # 7 p. 2580 - 2594
反应条件
lead(IV) acetate; N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran
T=25°C; 4 h;
参考文献
Wegmann, Helmut; Steglich, Wolfgang
Chemische Berichte, 1981 , vol. 114, # 7 p. 2580 - 2594
反应条件
lead(IV) acetate; N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran
T=25°C; 4 h;
参考文献
Wegmann, Helmut; Steglich, Wolfgang
Chemische Berichte, 1981 , vol. 114, # 7 p. 2580 - 2594
反应条件
lead(IV) acetate; N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran
T=25°C; 4 h;
参考文献
Wegmann, Helmut; Steglich, Wolfgang
Chemische Berichte, 1981 , vol. 114, # 7 p. 2580 - 2594
反应条件
lead(IV) acetate; N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran
T=25°C; 4 h;
参考文献
Wegmann, Helmut; Steglich, Wolfgang
Chemische Berichte, 1981 , vol. 114, # 7 p. 2580 - 2594
