3-甲基-2,3-二氢-1H-吲哚合成路线 （共 11 条）
反应条件
C21H21ClIrNO2 in tetrahydrofuran; 2,2,2-trifluoroethanol 20 h; Inert atmosphere;
参考文献
Wu, Jianjun; Talwar, Dinesh; Johnston, Steven; Yan, Ming; Xiao, Jianliang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., 2013 , vol. 125, # 27 p. 7121 - 7125,5
反应条件
oxygen; bis(3-methoxysalicylidene)ethylenediaminatocobalt(II) in methanol T=25°C; 4 h;
参考文献
Chemistry Letters, , p. 1287 - 1290
反应条件
in tetrahydrofuran 1 h;
参考文献
Tetrahedron, , vol. 41, # 21 p. 4727 - 4738
反应条件
nickel; decalin T=240 - 250°C; P=19000 Torr; Hydrogenation;
参考文献
v. Braun; Bayer; Blessing
Chemische Berichte, 1924 , vol. 57, p. 400
反应条件
T=240 - 250°C; P=19000 Torr; Hydrogenation;
参考文献
v. Braun; Bayer; Blessing
Chemische Berichte, 1924 , vol. 57, p. 400
反应条件
pyridine T=120°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Jiao, Lin-Yu; Oestreich, Martin
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 10845 - 10848
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=0 - 20°C;
参考文献
Pan, Shiguang; Ryu, Naoto; Shibata, Takanori
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 5 p. 929 - 933
反应条件
in tetrahydrofuran 1 h;
参考文献
Tetrahedron, , vol. 41, # 21 p. 4727 - 4738
反应条件
triethylamine in chloroform
T=0°C; 2 h;
参考文献
Neurogen Corporation
Patent: US6355644 B1, 2002 ;
Location in patent: Page column 23 ;
反应条件
in toluene
1 h; Heating / reflux;
参考文献
VERTEX PHARMACEUTICALS INCORPORATED
Patent: WO2006/10008 A1, 2006 ;
Location in patent: Page/Page column 175; 176-177 ;
WO 2006/010008 A1
