1,1-bis (3,5-di-t-butyl-4-hydroxyphenyl)-methane in toluene
T=190°C; 7 h;
参考文献
Mukmeneva, N. A.; Bukharov, S. V.; Kadyrova, V. Kh.; Zharkova, V. M.
Russian Journal of General Chemistry, 1994 , vol. 64, # 9.2 p. 1350 - 1351
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 9 p. 1507 - 1509
hydrogenchloride in tetrahydrofuran
treatment od reaction mixt. in THF with HCl soln., stirring (15 min); org. phase sepn., drying over Na2SO4 (24 h), soln. concn.; identification of individual compds.;
参考文献
Riviere, P.; Castel, A.; Abdennadher, C.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 82, # 1-4 p. 181 - 194
in tetrahydrofuran
org. compd. soln. addn. to excess Ge-compd., reaction mixt. filtration (celite) after 4 h at room temp.; filtrate concn. (reduced pressure); identification of individual compds.;
参考文献
Riviere, P.; Castel, A.; Abdennadher, C.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 82, # 1-4 p. 181 - 194
