2-庚基-1,3-二氧戊环合成路线 （共 19 条）
反应条件
in ethylene glycol; benzene
参考文献
Macro Chem. Corp.
Patent: US4861764 A1, 1989 ;
反应条件
hydroxylamine hydrochloride; toluene-4-sulfonic acid in ethanol
2 h; Heatingother aliphatic and aromatic acetals; without addition of TsOH and with HCl; MechanismProduct distribution;
参考文献
Yamauchi
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 11 p. 2042 - 2043
反应条件
tert.-butylhydroperoxide; Pd(OCOCF3)(OOBut) in benzene
T=50°C; 12 h;
参考文献
Hosokawa, Takahiro; Imada, Yasushi; Murahashi, Shun-Ichi
Journal of the Chemical Society, Chemical Communications, 1983 , # 21 p. 1245 - 1246
反应条件
oxygen; zinc(II) chloride; CoCl2 in ethylene glycol dimethyl ether
T=90°C; 30 h;
参考文献
Li, Pei; Alper, Howard
Canadian Journal of Chemistry, 1993 , vol. 71, # 1 p. 84 - 89
反应条件
water; iodine cloride in dichloromethane
0.5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Mingotaud; Florentin; Marquet
Synthetic Communications, 1992 , vol. 22, # 16 p. 2401 - 2404
反应条件
water; iodine cloride in acetonitrile
0.5 h; Ambient temperaturevar. oxidation agents and solvent; Product distribution;
参考文献
Mingotaud; Florentin; Marquet
Synthetic Communications, 1992 , vol. 22, # 16 p. 2401 - 2404
反应条件
water; iodine cloride in dichloromethane
0.5 h; Ambient temperature;
参考文献
Mingotaud; Florentin; Marquet
Synthetic Communications, 1992 , vol. 22, # 16 p. 2401 - 2404
反应条件
tetrabutylammomium bromide; bromine; ethylene glycol in dichloromethane
0.5 h; Yield given;
参考文献
Vasil'ev, A. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 6.1 p. 876 - 880
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 6 p. 822 - 826
反应条件
water; iodine cloride in dichloromethane
0.5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Mingotaud; Florentin; Marquet
Synthetic Communications, 1992 , vol. 22, # 16 p. 2401 - 2404
