2-乙基-2-苯基-1,3-二氧戊环合成路线 (共 7 条)
反应条件
tetrachlorosilane in dichloromethane T=20°C; 0.333333 h;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether T=30°C; Reduction; 12 h;
参考文献
Shaozu, Wu; Tianhui, Ren; Ning, Chen; Yulan, Zhang
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 427 - 431
反应条件
bromine in dichloromethane T=25 - 30°C; Bromination;
参考文献
Vasil'ev, Andrei; Engman, Lars
Journal of Organic Chemistry, 2000 , vol. 65, # 7 p. 2151 - 2162
反应条件
toluene-4-sulfonic acid in benzene
参考文献
Clark, George R.; Metzler, Michael R.; Whitaker, Giles; Woodgate, Paul D.
Journal of Organometallic Chemistry, 1996 , vol. 513, # 1-2 p. 109 - 134
反应条件
silver tetrafluoroborate; PPh3 gold(I) chloro complex in toluene
T=100°C; 3 h;
参考文献
Santos, Laura L.; Ruiz, Violeta R.; Sabater, Maria J.; Corma, Avelino
Tetrahedron, 2008 , vol. 64, # 34 p. 7902 - 7909
反应条件
Ambient temperatureIrradiationwithout cyclohexane but in DMSO; after previous adsorption at room temp. for 2 h on different zeolites forms prepared from the commercial 13X and LZY-52; Product distributionMechanism;
参考文献
Corma, Avelino; Garcia, Hermenegildo; Miranda, Miguel A.; Primo, Jaime; Sabater, Maria J.
Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6892 - 6894
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether
T=30°C; Reduction; 12 h;
参考文献
Shaozu, Wu; Tianhui, Ren; Ning, Chen; Yulan, Zhang
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 427 - 431