3H-萘并[2,1-b]吡喃-3-酮合成路线 (共 38 条)
反应条件
anhydrous iron chloride; silver trifluoromethanesulfonate; trifluoroacetic acid in 1,2-dichloro-ethane T=60°C; 15 h;
参考文献
Kutubi, Shahajahan; Hashimoto, Takuya; Kitamura, Tsugio
Synthesis, 2011 , # 8 art. no. F16111SS, p. 1283 - 1289
反应条件
tributylphosphine in methanol T=70°C; 20 h; Inert atmosphere;
参考文献
Boeck, Florian; Blazejak, Max; Anneser, Markus R.; Hintermann, Lukas
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 1630 - 1636,7
Title/Abstract Full Text Show Details
Boeck, Florian; Blazejak, Max; Anneser, Markus R.; Hintermann, Lukas
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 1630 - 1636
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; formic acid; sodium acetate T=25°C;
参考文献
Trost, Barry M.; Toste, F. Dean; Greenman, Kevin
Journal of the American Chemical Society, 2003 , vol. 125, # 15 p. 4518 - 4526
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane T=20°C; 8 h; Inert atmosphere;
参考文献
Hon, Yung-Son; Tseng, Tze-Wei; Cheng, Chia-Yi
Chemical Communications, 2009 , # 37 p. 5618 - 5620
反应条件
triethylamine; benzylamine in chloroform T=55°C; 48 h;
参考文献
Wei, Jia; Wang, Pengcheng; Jia, Qianfa; Huang, Jiaoyao; Du, Zhiyun; Zhang, Kun; Wang, Jian
European Journal of Organic Chemistry, 2013 , # 21 p. 4499 - 4502
反应条件
1: With RuCl2(tricyclohexylphosphine)2(benzylidene) in benzene T=40°C; 2 h; Inert atmosphere; 2: With tert.-butylhydroperoxide in decane; benzene 3.25 h; Inert atmosphere; regioselective reaction;
参考文献
Schmidt, Bernd; Krehl, Stefan
Chemical Communications, 2011 , vol. 47, # 20 p. 5879 - 5881
反应条件
pyrrolidine; copper(l) iodide in acetonitrile T=100°C; 2 h;
参考文献
Reddy, Maddi Sridhar; Thirupathi, Nuligonda; Haribabu, Madala
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 180 - 184
反应条件
palladium on activated charcoal in diphenylether 20 h; Heating;
参考文献
Panetta, Jill A.; Rapoport, Henry
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 946 - 950
反应条件
1: β-naphthol With [Pd(OAc)2(dppe)]; trifluoroacetic acid in dichloromethane T=0°C; 0.166667 h; 2: propynoic acid ethyl ester in dichloromethane T=0 - 30°C; 5 h;
参考文献
Kitamura, Tsugio; Tatemoto, Kotaro; Sakai, Mariko; Oyamada, Juzo
Chemistry Letters, 2012 , vol. 41, # 7 p. 705 - 707
反应条件
trifluorormethanesulfonic acid in toluene T=100°C; 2 h; Inert atmosphere;
参考文献
Hon, Yung-Son; Hong, Ya-Chun; Hong, Bor-Cherng; Liao, Ju-Hsiou
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 3 p. 407 - 420