3-甲基-3-吡唑啉-5-酮合成路线 (共 38 条)
反应条件
hydrazine in neat (no solvent) T=140°C; 0.00555556 h; IrradiationGreen chemistry; Reagent/catalyst;
参考文献
Dandia, Anshu; Parewa, Vijay; Gupta, Shyam L.; Rathore, Kuldeep S.
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 373, p. 61 - 71
反应条件
hydrazine in ethanol T=20°C; 16 h;
参考文献
Jung, Jae-Chul; Watkins, E.Blake; Avery, Mitchell A
Tetrahedron, 2002 , vol. 58, # 18 p. 3639 - 3646
反应条件
hydrazine hydrate in ethanol T=150°C; 5 h;
参考文献
Bisenieks; Uldrikis; Duburs
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 7 p. 869 - 875
反应条件
1: With hydroxymethyl polystyrene resin in toluene T=100°C; 4 h; 2: With hydrazine in ethanol
参考文献
Yamazaki, Kazuo; Nakamura, Yosuke; Kondo, Yoshinori
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 6011 - 6019
反应条件
sulfuric acid in ethanol 0.5 h; Heating;
参考文献
Jonsson; Kristinsson; Nussbaumer; Skulason; Winkler
Synthesis, 1995 , # 7 p. 805 - 809
反应条件
hydrazine hydrate in ethanol T=150°C; 5 h;
参考文献
Bisenieks; Uldrikis; Duburs
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 7 p. 869 - 875
反应条件
ethanol; hydrazine hydrate T=120°C; im Rohr;
参考文献
v. Rothenburg
Chemische Berichte, 1894 , vol. 27, p. 791
Journal fuer Praktische Chemie (Leipzig), 1895 , vol. <2> 51, p. 61
反应条件
sulfuric acid T=140 - 150°C;
参考文献
Wolff
Chemische Berichte, 1904 , vol. 37, p. 2830
Chemische Berichte, 1905 , vol. 38, p. 3039
反应条件
hydrazine hydrate in ethanol 0.333333 h; Heating; Yield given. Yields of byproduct given;
参考文献
Yogo, Motoi; Hirota, Kosaku; Senda,Shigeo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 473 - 475
反应条件
hydrazine in ethanol
参考文献
Benchidmi, M.; Essassi, E. M.; Ibnmansour, A.
Bulletin des Societes Chimiques Belges, 1992 , vol. 101, # 12 p. 995 - 1000