氨基亚氨基硫代甲基氢碘酸合成路线 （共 25 条）
反应条件
in ethanol T=20°C; 12 h;
参考文献
Aoyagi, Naoto; Furusho, Yoshio; Endo, Takeshi
Synlett, 2014 , vol. 25, # 7 art. no. 6650, p. 983 - 986
反应条件
1: With triethylamine in water T=20 - 50°C; 18.4167 h; 2: With hydrogenchloride; water T=0 - 5°C; pH=2;
参考文献
F. HOFFMANN-LA ROCHE AG
Patent: WO2007/88014 A1, 2007 ;
Location in patent: Page/Page column 30-31 ;
WO 2007/088014 A1
反应条件
sodium ethanolate in ethanol 1.) RT, 1 h, 2.) reflux, 20 h;
参考文献
Takagi, K.; Bajnati, A.; Hubert-Habart, M.
Bulletin de la Societe Chimique de France, 1990 , # 5 p. 660 - 666
参考文献
Derocque,J.-L. et al.
Bulletin de la Societe Chimique de France, 1968 , p. 2062 - 2066
参考文献
Klayman,D.L. et al.
Journal of Medicinal Chemistry, 1969 , vol. 12, p. 723 - 725
反应条件
sodium in ethanol 0 deg C, 15 min, 0 deg C to RT, reflux, 1 h;
参考文献
Bajnati, Abdelilah; Kokel, Bruno; Hubert-Habart, Michel
Bulletin de la Societe Chimique de France, 1987 , # 2 p. 318 - 324
参考文献
Bernthsen; Klinger
Chemische Berichte, 1878 , vol. 11, p. 493
参考文献
Bernthsen; Klinger
Chemische Berichte, 1878 , vol. 11, p. 493
反应条件
sodium in ethanol 0 deg C, 15 min, 0 deg C to RT, reflux, 1 h;
参考文献
Bajnati, Abdelilah; Kokel, Bruno; Hubert-Habart, Michel
Bulletin de la Societe Chimique de France, 1987 , # 2 p. 318 - 324
反应条件
sodium hydrogen selenide in ethanol
参考文献
Journal of Organic Chemistry, , vol. 34, p. 3549 - 3551
