1-Alpha-氯-3,5-二-O-对甲苯甲酰基-2-脱氧-D-呋喃核糖合成路线 （共 54 条）
反应条件
acetyl chloride in acetic acid T=20°C;
参考文献
McKeen, Catherine M.; Brown, Lynda J.; Nicol, Jamie T.G.; Mellor, John M.; Brown, Tom
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 13 p. 2267 - 2275
反应条件
hydrogenchloride in diethyl ether T=0°C; 0.166667 h;
参考文献
Ogino, Masayuki; Yoshimura, Yoshinaga; Nakazawa, Akio; Saito, Isao; Fujimoto, Kenzo
Organic Letters, 2005 , vol. 7, # 14 p. 2853 - 2856
反应条件
1.1: AcCl / 2 h / 20 °C 1.2: DMAP; pyridine / 12 h / 0 °C 2.1: 72 percent / HCl gas / diethyl ether / 0.17 h / 0 °C View Scheme
参考文献
Koegler, Martin; Busson, Roger; De Jonghe, Steven; Rozenski, Jef; Van Belle, Kristien; Louat, Thierry; Munier-Lehmann, Helne; Herdewijn, Piet
Chemistry and Biodiversity, 2012 , vol. 9, # 3 p. 536 - 556
反应条件
1: 2-deoxy-D-ribofuranose With acetyl chloride in methanol T=20°C; 1.16667 h; Inert atmosphere; 2: 4-methyl-benzoyl chloride With pyridine in methanol T=0 - 20°C; Inert atmosphere; 3: With acetic acid; acetyl chloride in methanol T=0°C; Inert atmosphere;
参考文献
Dierckx, Anke; Miannay, Francois-Alexandre; Ben Gaied, Nouha; Preus, Soren; Bjoerck, Markus; Brown, Tom; Wilhelmsson, L. Marcus
Chemistry - A European Journal, 2012 , vol. 18, # 19 p. 5987 - 5997
反应条件
hydrogenchloride; acetic acid
参考文献
Hoffer et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4112
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Hoffer
Chemische Berichte, 1960 , vol. 93, p. 2777,2780
反应条件
1.1: AcCl / 2 h / 20 °C 1.2: DMAP; pyridine / 12 h / 0 °C 2.1: 72 percent / HCl gas / diethyl ether / 0.17 h / 0 °C View Scheme
参考文献
Dhimitruka, Ilirian; SantaLucia Jr., John
Synlett, 2004 , # 2 p. 335 - 337
反应条件
1: 90 percent / NaH / tetrahydrofuran / 4 h / 60 - 70 °C 2: HCl / diethyl ether View Scheme
参考文献
Dhimitruka, Ilirian; SantaLucia Jr., John
Synlett, 2004 , # 2 p. 335 - 337
反应条件
1: HCl / 0.42 h / Ambient temperature 2: pyridine / Ambient temperature 3: HCl View Scheme
参考文献
Rolland, Valerie; Kotera, Mitsuharu; Lhomme, Jean
Synthetic Communications, 1997 , vol. 27, # 20 p. 3505 - 3511
反应条件
1: 95 percent / NaH / acetonitrile; CH2Cl2 / 5 h / 0 - 20 °C 2: 830 mg / NaI / acetonitrile / 1.5 h / 60 °C 3: 100 percent / NH3 / methanol / 11 h / 60 °C View Scheme
参考文献
Kazimierczuk, Zygmunt; Cottam, Howard B.; Revankar, Ganapathi R.; Robins, Roland K.
Journal of the American Chemical Society, 1984 , vol. 106, # 21 p. 6379 - 6382
反应条件
ammonia; sodium hydride Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Worthington, Victoria L.; Fraser, William; Schwalbe, Carl H.
Carbohydrate Research, 1995 , vol. 275, # 2 p. 275 - 284
