1-乙氧基-2,2,2-三氟乙醇合成路线 （共 58 条）
反应条件
in toluene 64 h; Reflux;
参考文献
Kenis, Sara; D'Hooghe, Matthias; Verniest, Guido; Reybroeck, Maaike; Dang Thi, Tuyet Anh; Pham The, Chinh; Thi Pham, Tham; Toernroos, Karl W.; Van Tuyen, Nguyen; De Kimpe, Norbert
Chemistry - A European Journal, 2013 , vol. 19, # 19 p. 5966 - 5971
反应条件
titanium tetrachloride in dichloromethane 24 h; Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 93, # 2 p. 165 - 170
参考文献
Journal of Medicinal Chemistry, , vol. 41, # 8 p. 1315 - 1343
反应条件
1: trifluoroacetaldehyde ethyl hemiacetal With sulfuric acid T=70 - 150°C; 0.133333 h; microwave irradiation; 2: Bromure de phenyl magnesium in diethyl ether T=20°C; Grignard reaction; 0.25 h; Further stages.;
参考文献
Landge, Shainaz M.; Borkin, Dmitry A.; Toeroek, Bela
Tetrahedron Letters, 2007 , vol. 48, # 36 p. 6372 - 6376
反应条件
aluminium trichloride in 1,2-dichloro-ethane 16 h; Ambient temperature; Yield given;
参考文献
Guy, A.; Lobgeois, A.; Lemaire, M.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 361 - 366
反应条件
iron(III) chloride in 1,2-dichloro-ethane 16 h; Ambient temperaturevariation of catalyst and solvent; Product distribution;
参考文献
Guy, A.; Lobgeois, A.; Lemaire, M.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 361 - 366
反应条件
1: trifluoroacetaldehyde ethyl hemiacetal With sulfuric acid T=70 - 150°C; 0.133333 h; microwave irradiation; 2: Bromure de phenyl magnesium in diethyl ether T=20°C; Grignard reaction; 0.25 h; Further stages.;
参考文献
Landge, Shainaz M.; Borkin, Dmitry A.; Toeroek, Bela
Tetrahedron Letters, 2007 , vol. 48, # 36 p. 6372 - 6376
反应条件
aluminium trichloride in 1,2-dichloro-ethane 16 h; Ambient temperature; Yield given;
参考文献
Guy, A.; Lobgeois, A.; Lemaire, M.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 361 - 366
反应条件
iron(III) chloride in 1,2-dichloro-ethane 16 h; Ambient temperaturevariation of catalyst and solvent; Product distribution;
参考文献
Guy, A.; Lobgeois, A.; Lemaire, M.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 361 - 366
参考文献
Ito, Hisanaka; Sato, Azusa; Kobayashi, Tetsuo; Taguchi, Takeo
Chemical Communications, 1998 , # 22 p. 2441 - 2442
