二(1-苯并三唑基)甲硫酮合成路线 (共 20 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 4 h; Heating;
参考文献
Tiwari, Vinod K.; Singh, Desh D.; Hussain, Hakkim A.; Mishra, Bhuwan B.; Singh, Archana
Monatshefte fur Chemie, 2008 , vol. 139, # 1 p. 43 - 48
反应条件
1: triethylamine / dichloromethane / 0.17 h / 20 °C / |Inert atmosphere 2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.23 h / 110 °C / |Inert atmosphere View Scheme
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 3 h; Heating;
参考文献
Tiwari, Vinod K.; Singh, Desh D.; Hussain, Hakkim A.; Mishra, Bhuwan B.; Singh, Archana
Monatshefte fur Chemie, 2008 , vol. 139, # 1 p. 43 - 48
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
参考文献
Kale, Raju R.; Prasad, Virendra; Tiwari, Vinod K.
Synlett, 2011 , # 2 art. no. G31010ST, p. 195 - 198
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 3 h; Heating;
参考文献
Tiwari, Vinod K.; Singh, Desh D.; Hussain, Hakkim A.; Mishra, Bhuwan B.; Singh, Archana
Monatshefte fur Chemie, 2008 , vol. 139, # 1 p. 43 - 48
反应条件
in dichloromethane T=20°C; 18 h;
参考文献
Katritzky, Alan R.; Witek, Rachel M.; Rodriguez-Garcia, Valerie; Mohapatra, Prabhu P.; Rogers, James W.; Cusido, Janet; Abdel-Fattah, Ashraf A. A.; Steel, Peter J.
Journal of Organic Chemistry, 2005 , vol. 70, # 20 p. 7866 - 7881
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
参考文献
Kale, Raju R.; Prasad, Virendra; Tiwari, Vinod K.
Synlett, 2011 , # 2 art. no. G31010ST, p. 195 - 198
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 3 h; Heating;
参考文献
Tiwari, Vinod K.; Singh, Desh D.; Hussain, Hakkim A.; Mishra, Bhuwan B.; Singh, Archana
Monatshefte fur Chemie, 2008 , vol. 139, # 1 p. 43 - 48
反应条件
1: pyridine / dichloromethane / 0 °C / |Inert atmosphere
2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.33 h / 110 °C / |Inert atmosphere
View Scheme
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
反应条件
in tetrahydrofuran
5 h; Heating;
参考文献
Katritzky, Alan R.; Witek, Rachel M.; Rodriguez-Garcia, Valerie; Mohapatra, Prabhu P.; Rogers, James W.; Cusido, Janet; Abdel-Fattah, Ashraf A. A.; Steel, Peter J.
Journal of Organic Chemistry, 2005 , vol. 70, # 20 p. 7866 - 7881