1-环己基-3-苯基-1-丙酮合成路线 (共 21 条)
反应条件
sodium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride in water T=185°C; P=7600 Torr; microwave irradiation;
参考文献
Ishibashi, Kenichi; Takahashi, Masaaki; Yokota, Yutaka; Oshima, Koichiro; Matsubara, Seijiro
Chemistry Letters, 2005 , vol. 34, # 5 p. 664 - 665
反应条件
barium hydroxide monohydrate; water; palladium nanoparticles in poly(viologen) T=100°C; 24 h;
参考文献
Yamada, Yoichi M.A.; Uozumi, Yasuhiro
Tetrahedron, 2007 , vol. 63, # 35 p. 8492 - 8498
反应条件
oxygen; palladium diacetate; acetic acid; copper(l) chloride in dimethyl sulfoxide T=50°C; P=760.051 Torr; 20 h; regioselective reaction;
参考文献
Chen, Mao; Wang, Jie; Chai, Ziyi; You, Cai; Lei, Aiwen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 341 - 346
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 2Br(1-)*C30H47BrN4(2+); potassium tert-butylate; hydrogen in para-xylene T=125°C; P=760.051 Torr;
参考文献
Kose, Osamu; Saito, Susumu
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 4 p. 896 - 900
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; P=60800 Torr; 3 h;
参考文献
Ryu, Ilhyong; Kusano, Kazuya; Yamazaki, Hiroshi; Sonoda, Noboru
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5003 - 5005
反应条件
Grignard reagent; N,N-diphenyl-p-methoxyphenylchloromethyleniminium chloride; copper(l) iodide in tetrahydrofuran; dichloromethane 1) -30 deg C, 1 h, 2) 0 deg C, 1 h;
参考文献
Fujisawa, Tamotsu; Mori, Toshiki; Sato, Toshio
Tetrahedron Letters, 1982 , vol. 23, # 48 p. 5059 - 5062
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C;
参考文献
Boger, Dale L.; Mathvink, Robert J.
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1429 - 1443
反应条件
chromium(VI) oxide; sulfuric acid in water; acetone cooling;
参考文献
Ema, Tadashi; Ura, Norichika; Yoshii, Masataka; Korenaga, Toshinobu; Sakai, Takashi
Tetrahedron, 2009 , vol. 65, # 46 p. 9583 - 9591
反应条件
hydrogenchloride in tetrahydrofuran; diethyl ether T=20°C; 10 h; Yield given;
参考文献
Katritzky, Alan R.; Zhang, Guifen; Jiang, Jinlong
Journal of Organic Chemistry, 1995 , vol. 60, # 23 p. 7605 - 7611
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Boger, Dale L.; Mathvink, Robert J.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1777 - 1779